A-Level Chemistry: Mass Spectrometry Syllabus

This page summarises the main mass spectrometry content commonly covered in UK A-Level Chemistry. It focuses on what students are generally expected to know for exam purposes.

What mass spectrometry is used for

  • Finding relative isotopic mass.
  • Finding the relative abundance of isotopes.
  • Calculating relative atomic mass.
  • Determining relative molecular mass (Mr).
  • Helping identify simple organic compounds from fragmentation patterns.

Key knowledge students should learn

  • How to read simple mass spectra of elements.
  • How to use isotope abundances to calculate relative atomic mass.
  • How to identify the molecular ion peak.
  • How to use the m/z value to interpret spectra.
  • How fragmentation produces smaller peaks that give clues about structure.

Time-of-flight mass spectrometry

For some exam boards, especially AQA, students are expected to know the basic stages of a time-of-flight (TOF) mass spectrometer:

  • Ionisation
  • Acceleration
  • Ion drift
  • Detection
  • Data analysis

Board differences at a glance

AQA

Emphasises TOF principles, isotopes, simple spectra of elements, and using mass spectrometry to determine relative molecular mass.

Edexcel

Includes isotopes and Mr, plus molecular ion peaks, fragmentation, and accurate mass in analytical topics.

OCR

Places mass spectrometry within analytical techniques, including isotope calculations, fragmentation analysis, and structure deduction.

Typical exam-style tasks

  • Calculate Ar from isotopic abundance data.
  • Identify the molecular ion peak.
  • Determine the Mr of a compound.
  • Explain why peaks appear at different m/z values.
  • Use fragmentation peaks to suggest a simple structure.

Sources